Professor Kenneth R. Poeppelmeier
Charles E. & Emma H. Morrison Professor of Chemistry
Rm: Tech GG35Ph: 847-491-3505 |
BS,
University of Missouri PhD, Iowa State University Associate Editor, Inorganic Chemistry Associate Director, Northwestern University Science and Technology Center for Superconductivity Editorial Boards, Journal of Alloys and Compounds, CHEMtracks, Chemistry of Materials, Solid State Sciences Lecturer, National Science Council of Taiwan Fellow, Japan Society for the Promotion of Science Fellow, American Association for the Advancement of Science Chair, American Chemical Society Division of Inorganic Chemistry & Solid-State Chemistry Lecturer, Natural Science Foundation of China |
Inorganic solid-state chemistry has always had widespread use in industrial applications and in diverse fields such as heterogeneous catalysis and ceramics. Our research emphasizes the connections between the synthesis and structure of new materials, the physical properties of new materials, and the technological advances that can result from these discoveries.
One specific example of this is our development of Ag4V2O6F2
(SVOF) as a primary lithium battery material. Presently, Ag2V4O11,
or silver
vanadium oxide (SVO), is used commercially as a cathode material in
primary lithium batteries for high-rate applications, such as those
used in implantable cardioverter defibrillators (ICDs). An ICD monitors
the heartbeat and, when arrhythmia is detected, interrupts the
fibrillation by delivering a shock of 30-35 J to the heart to restore
normal rhythm. To deliver the shock, capacitors are rapidly charged to
a high voltage and then discharged directly into the heart via
electrical leads. SVOF has a higher silver-to-vanadium ratio than SVO,
while preserving critical connectivity in the vanadium oxide fluoride
framework. The silver ions lie between sheets of alternating vanadium
tetrahedra and octahedra chains. This silver interlayer between the
vanadium oxide fluoride sheets allows for lithium diffusion into the
material and silver diffusion out of the material. An open circuit
voltage experiment, which clarifies the voltage plateaus of the
electrode, shows the first plateau is at 3.52 V and the second is at
3.25 V. The initial voltage plateau is nearly 300 mV higher than the
silver reduction potential of SVO. In addition to the higher reduction
potential, the capacity of SVOF above 3 V is 148 mAh/g (892 mAh/cm3),
equivalent
to
3.7
mol
of
lithium
inserted,
while
SVO
has
a
capacity
of
100
mAh/g
(480
mAh/cm3). Thus, it is apparent that the
presence of the fluoride increases the reduction potential of the
silver and the greater silver content increases the capacity at higher
voltages.
Inorganic materials that have unusual structures often exhibit interesting chemical and physical characteristics. For example, layered materials exhibit a wide variety of important technological uses because they offer a unique crystalline architecture that can be designed to achieve specific material properties. Most recently, we have begun synthesizing and testing novel mixed metal ferrites as solid oxide fuel cell electrodes, while also studying the fundamental relationship between the structure and its properties. We are also interested in noncentrosymmetric compounds and their technologically important properties such as ferroelectricity and second-order nonlinear behavior. More recently we have begun to study metal oxides that are transparent throughout the visible range yet are metallic conductors. Our research in these areas, ranging from growth of single crystals to the synthesis of new catalysts, is part of an interdisciplinary research program that involves the collaboration of physicists, materials scientists, and chemists.
Selected Publications
"The Role of Polar, Lamdba (Λ)-Shaped Building Units in Noncentrosymmetric Inorganic Structures" (Cover article), M. D. Donakowski, R. Gautier, J. Yeon, D. T. Moore, J. C. Nino, P. S. Halasymani, K. R. Poeppelmeier, J. Amer. Chem. Soc., 2012, 134, 7679.
"Structural, Optical, and Transport Properties of a- and ß-Ag3VO4", V. Cloet, A. Raw, K. R. Poeppelmeier, G. Trimarchi, H. Peng, J. Im, A. J. Freeman, N. H. Perry, T. O. Mason, A. Zakutayev, P. F. Ndione, D. S. Ginley, J. D. Perkins, Chem. Mat., 2012, 24, 3346-3354.
"A Chemical Approach to Understanding Oxide Surfaces", J. A. Enterkin, K. R. Poeppelmeier, and L. D. Marks, Surf. Sci., 2012, 606, 344-355.
"Orientational Order of [VOF5]2- and [NbOF5]2- Polar Units in Chains", R. Gautier, M. D. Donakowski, K. R. Poeppelmeier, J. Solid State Chem., 2012, 195, 132-139.
"Ionothermal Synthesis: A New Spin on Frustration", K. R. Poeppelmeier and M. Azuma, Nature Chemistry, 2011, 3, 758-759.[PDF]
"K3B6O10Cl: A New Structure Analogous to Perovskite with a Large Second Harmonic Generation Response and Deep UV Absorption Edge", H. Wu, S. Pan, K. R. Poeppelmeier, H. Li, D. Jia, Z. Chen, X. Fan, Y. Yang, J. M. Rondinelli, H. Luo, 2011, J. Am. Chem. Soc., 133, 7786-7790. [PDF]
"High-Pressure Synthesis and Local Structure of Corundum-Type In2-2xZnxSnxO3 (x = 0.7)", C. A. Hoel, J. M. Gallardo Amores, E. Morán, M. A. Alario-Franco, J.-F. Gaillard, and K. R. Poeppelmeier, 2010, J. Am. Chem. Soc., 132, 16479-16487. [PDF]
"Ternary and Multinary Materials: Crystal/Defect Structure-Property Relationships", T. O. Mason, S. P. Harvey, and K. R. Poeppelmeier 2010, Handbook of Transparent Conductors, D. S. Ginley et al. Eds., Pringer Science+Business Media, LLC, Chapter 8, p. 265-293.
"Structural and Chemical Evolution of the SOFC Anode La0.30Sr0.70Fe0.70Cr0.30O3-d upon Reduction and Oxidation: An In-Situ Neutron Diffraction Study", H. Haag, S, Barnett, J. Richardson, K. R. Poeppelmeier, 2010, Chem. Mater., 22, 3283-3289. [PDF]
"A Homologous Series of Structures on the Surface of SrTiO3(110)", J. A. Enterkin, A. Subramanian, B. Russell, M. Castell, K. R. Poeppelmeier, and L. Marks, 2010, Nature Mat., 9, 245-248. [PDF]
"Chemical Hardness and the Adaptive Coordination Behavior of the d0 Transition Metal Oxide Fluoride Anions", M. R. Marvel, R. A. F. Pinlac, J. Lesage, C. L. Stern, and K. R. Poeppelmeier, 2009, Z. Anorg. Allg. Chem., 635, 869-877. [PDF]
"Cation-Anion Interactions and Polar Structures in the Solid State",
M. Marvel, J. Lesage, J. Baek, P. S. Halasyamani, C. L. Stern, and K. Poeppelmeier, J. Am. Chem. Soc., 2007, 129, 13963-13969.
[PDF]
"Hydrothermal
Synthesis
of
Delafossite-Type
Oxides",
Sheets,
W.
C.,
Mugnier,
E.,
Barnabe,
A.,
Marks,
T.
J.,
Poeppelmeier,
K.
R.
Chem. Mater., 2006 18, 7-20.
[PDF]
"Probing
the
Vanadyl
and
Molybdenyl
Bonds
in
Complex
Vanadomolybdate
Structures",
Smit,
J.
P.,
Kim,
H.-S.,
Pless,
J.
D.,
Stair,
P. C., Poeppelmeier, K.
R. Inorg. Chem., 2006 45, 521-528.
[PDF]
"Synthesis,
Crystal
Structure,
and
Nonlinear
Optical
Properties
of
Li6CuB4O10:
A
Congruently
Melting
Compound with Isolated [CuB4O10]6-
Units",
Pan, S., Smit, J. P., Watkins, B., Marvel, M. R., Stern, C. L.,
Poeppelmeier, K. R. J. Am. Chem. Soc., 2006, 128,
11631-11634.
[PDF]
"Ag4V2O6F2:
An
Electrochemically
Active
and
High
Silver
Density
Phase",
Sorensen,
E.
M.,
Izumi,
H.
K.,
Vaughey,
J.
T.,
Stern, C. L.,
Poeppelmeier, K. R.
J. Am. Chem. Soc., 2005, 127(17), 6347-6352.
[PDF]
"Catalytic
Oxidative
Dehydrogenation
of
Propane
over
Mg-V/Mo
Oxides",
Pless,
J.
D.,
Bardin,
B.
B.,
Kim,
H.-S.,
Ko,
D.,
Smith, M. T.,
Hammond, R. R., Stair, P. C., Poeppelmeier, K. P.J. Catal., 2004,
223,
419-431.
[PDF]
"Single
Crystal
Growth
of
Magnesium
Orthovanadate,
Mg3(VO4)2,
by
the
Optical Floating Zone Technique", Pless, J. D., Erdman, N., Ko, D.,
Marks, L. D., Stair, P. C., Poeppelmeier, K. R. Cryst. Growth Des.,
2003, 3, 615-619.
[PDF]
"The
ordered [WO2F4]2- anion",
Welk, M.E., Norquist, A.J., Stern, C.L., Poeppelmeier, K.R. Inorg.
Chem. 2001, 40, 5479-5480.
[PDF]
"A high yield hydrothermal preparation of CuAlO2",
Shahriari, D.Y., Barnabe, A., Mason, T.O., Poeppelmeier, K.R.
Inorg. Chem., 2001, 40, 5734-5735.
[PDF]
| 1985-1989
| 1990-1994
| 1995-2000
| 2001-2005
| 2006-2010
| 2011-2015
| 2016-Present
| Old Group Photos
|
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Tel: +81-3-5841-7777
Fax: +81-3-5689-0574
email: otzschi@sogo.t.u-tokyo.ac.jp
Dr. George B. Palmer (PhD 1999)
McKinsey & Company, Inc.
Suite 4600, Georgia-Pacific Center
133 Peachtree Street, N.E.
Atlanta, Georgia 30303
Tel: (404) 335-3846
Fax: (404) 521-1743
Email: george_palmer@mckinsey.com
Dr. Paul Salvador (PhD 2/1997)
Assistant Professor
Carnegie Mellon University
Department of Materials Science and Engineering
Rm 3301 Wean Hall
5000 Forbes Avenue
Pittsburgh, PA 15213-2890
Tel: (412) 268-2702
Fax: (412) 268-7596
email: paul7@andrew.cmu.edu
Professor Douglas Vander Griend (Ph.D. 9/00)
Department of Chemistry & Biochemistry
Calvin College
Grand Rapids, MI 49546
Tel: (616)957-8729
Fax: (616)957-6501
email: dvg@calvin.edu
Michael J. Willis 1996
President
Admiral Chemicals
6200 N. 39th Street
Milwaukee, WI 53201 USA
Tel: 1 (414) 286-1070
email: mike.willis@admiralchemicals.com
Dr. Alexandre Wahl
Laboratoire CRISMAT - ISMRA
6 Bd Maréchal Juin
14050 CAEN Cedex
France
Tel : 02 31 45 29 13
Fax : 02 31 95 16 00
e-mail : Alexandre.wahl@ensicaen.fr
Dr. Xiandong Wang
Gillette Advanced Technology Center
37 A Street
Needham, MA 02492
Tel: 781-292-8620
Fax: 781-292-8615
email: Xiandong_Wang@gillette.com
Dr. Jan Allen (PhD 1993)
Sensors and Electron Devices Directorate
Attn: AMSRL-SE-DC
2800 Powder Mill Road
Adelphi, MD 20783?1197
Tel: 301-394-0291
Fax: 301-394-0273
email: jallen@arl.army.mil
Dr. Mark Anderson (PhD 1992)
Ceramic Technology Center
Industrial and Consumer Sector Research Laboratory
3M Center, Building 201-4N-01
St. Paul, MN 55144-1000
Tel: 612-737-2570
Fax: 612-737-4682
email: mtanderson@mmm.com
Dr. Gordon Bain (PhD 1994)
General Chemistry Lab Director (7/2000)
Department of Chemistry
University of Wisconsin - Madison
1101 University Avenue
Madison, WI 53706
Tel: (608) 263-4581
email: bain@chem.wisc.edu
Dr. Dawn Groenke (PhD 1994)
5 Brevard Court (6/98)
Durham, NC 27713
email: dagroen@aol.com
Dr. Mark Kennard (PhD 1993)
Lam Research Corporation
4650 Chushing Parkway
Fremont, CA 94538-6401
Tel: 510-572-8558
Fax: 510-572-5515
email: mark.kennard@lamrc.com
Dr. Steve Mayorga (PhD 90-91)
Air Products and Chemicals, Inc.
7201 Hamilton Boulevard
Allentown, PA 18195-1501
Tel: 215-481-2499
email: mayorgsg@apci.com
Ken Rogers (MS 95)
Northwest Representative
Molecular BioProducts
9880 Mesa Rim Road
San Diego, CA 92121
Fax: 415 242 9520
email: magik1@sprynet.com
Dr. James P. Thiel (PhD 1991)
Department of Chemistry
The University of Oregon
Eugene, Oregon 97403
Tel: 503-346-4601
Fax: 503-346-4643
Dr. Steve Thong (PhD 1990)
Manager, New Technology Group
The Gillette Company
One Gillette Park
Boston, MA 02127-1096
Tel: (617) 463-2802 (W)
Fax: (617) 463-2212
email: Stephen_Thong@gillette.com
Dr. Douglas Tomczak (PhD 1993)
Senior Project Chemist
Unilever
Rolling Meadows, IL
email: Douglas.Tomczak@unilever.com
Dr. Robert Toreki (PD 93)
Department of Chemistry
Chemistry-Physics Bldg.
University of Kentucky, Lexington, KY 40506-0055
Tel: 606-257-7073
email: rtore00@ukcc.uky.edu
Dr. Jack Vaughey (PhD 1992)
Argonne National Lab
CMT-Chemical Technology Division
9700 S. Cass Avenue
Argonne, IL 60439
Phone: 630-252-8885 or 630-252-4672
Fax: 630-252-4176
email: vaughey@cmt.anl.gov
Dr. Cyril C. K. Chiang (PhD 1989)
Mobile: +886-930-857071
email: cyril.chiang@msa.hinet.net
Professor Shiou-Jyh Hwu (PhD 1988)
Clemson University
Department of Chemistry
477 Howard Hunter Chemistry Laboratory
Box 341905
Clemson, SC 29634-1905
Tel: 803-656-5031
Fax: 803-656-6613
email: shwu@clemson.edu
webpage: chemistry.clemson.edu/people/hwu.htm
Dr. Dale O. Kipp (PhD 1988)
Director, MatWeb Divison Automation Creations, Inc.
2000 Kraft Drive, Suite
Blacksburg, VA 24060-6373
Tel: 540-552-5300
Fax: 540-552-1657
email: dale@matls.com
Dr. Lorraine Townsend (PhD 1989) (12/94)
Du Pont, Yerkes Plant
P.O. Box 88
Buffalo, NY 14207
Tel:(716) 879-4623
email: Lorraine.A.Townsend@usa.dupont.com
Dr. John B. Wiley (PhD 1989)
Department of Chemistry
University of New Orleans
New Orleans, LA 70148
Tel: 504-286-6849 (office); 504-286-5569 (Lab)
Fax: 504-280-6860
email: jwiley@uno.edu
webpage: www.chem.uno.edu/Wiley.html